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1 article(s) from Sato, Eisuke

Electrochemical hydrogenation of enones using a proton-exchange membrane reactor: selectivity and utility

Koichi Mitsudo,
Haruka Inoue,
Yuta Niki,
Eisuke Sato and
Seiji Suga

Beilstein J. Org. Chem. 2022, 18, 1055–1061, doi:10.3762/bjoc.18.107

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Scheme 1: Designed electrochemical hydrogenation of enones 1 with a PEM reactor.

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Figure 1: Electrochemical setup of the PEM reactor: a) Electrochemical reduction system with the PEM reactor....

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Figure 2: Reaction profile of the electrochemical hydrogenation of 1a with a PEM reactor using a) Pd/C and b)...

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Scheme 2: Electrochemical hydrogenation of several enones 1 with a circulating PEM reactor using a Pd/C catho...

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Scheme 3: Electrochemical hydrogenation of several enones 1 with a circulating PEM reactor using an Ir/C cath...

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Scheme 4: Mechanistic studies.

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Scheme 5: Electroreduction of 1a with the circulating PEM reactor using H₂O as a proton source.

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Published 19 Aug 2022

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